Course code:
2351H		 Course name:
Selected Methods of Instrumental Analysis

Academic year:

2012/2013.

Attendance requirements:

There are no requirements.

ECTS:

8

Study level:

graduate academic studies

Study program:

Chemistry: 1. year, winter semester, elective (2IP1H) course

Teachers:

Rada M. Baošić, Ph.D.
full professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Dragan D. Manojlović, Ph.D.
full professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Assistant:

Jelena J. Mutić, Ph.D.
full professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Hours of instruction:

Weekly: four hours of lectures + two hours of exercises + three hours of labwork (4+2+3)

Goals:

The aim of the course is that student complete their theoretical and practical knowledge from these methods and to qualify him for independent research in this field. In addition, students will complete their knowledge in the field of sensors, nanosenzora, analysis and characterization of surfaces and materials analysis and characterization of powders.Within the scope of the course students will acquire theoretical and practical knowledge in the field of application of instrumental methods in speciation species in environmental chemistry and the possibilities of determining different oxidation statesof certain species.

Outcome:

Student will be qualified for independent research, optimisation and improving sensitivity of instrumental methods for the analysis of complex samples.

Teaching methods:

Lectures, labworks.

Extracurricular activities:

—

Coursebooks:

Main coursebooks:

  1. David Harvey, Modern Analytical Chemistry, McGraw-Hill Higer Education, 2000.
  2. A. J. Bard, L. R. Faulkner, Electrochemical methods Fundamentals and applications, Wiley, 2000.

Supplementary coursebooks:

  1. H. Girault, Analytical and phisical electrochemistry, EPEL Press, 2004.
  2. A. M. Ure and C.M. Davidson, Chemical speciation in the environment, Blackwell Science, 2002.
  3. G. Bendre, Principle of Chemical Instrumentation, W.B. Saunder Company, Philadelphia, 1987.

Additional material:

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  Course activities and grading method

Lectures:

5 points (4 hours a week)

Syllabus:

  • Electrochemical potential, Electrochemical equilibria.
  • Investigation og electrode rections (cyclic voltammetry and spectroelectrochemistry).
  • SECM (scanning electrochemical microscopy).
  • Electrochemical biosensors, miniaturization (nanosensors).
  • Puls techniques, Striping analysis.
  • Practical aspects (electrochemical cell, chemical modification of electrodes).
  • Electrochemical methods of separation.
  • Modern optical methods, introduction and classification.
  • Spectroscopic instruments.
  • Atomic emission spectrometry.
  • Atomic absorption spectrometry..
  • Atomic fluorescence spectrometry
  • Laser enhanced ionisation spectroscopy
  • Electronic microscopy. Optical sensors.
  • Semester paper.
  • Hybride techniques (ICP-MS, GC-AAS, GC-ICP, GC-MS, HPLC-ICP).
  • Application of instrumental methods in environmental chemistry and possibilities of speciation of species.

Exercises:

0 points (2 hours a week)

Labwork:

20 points (3 hours a week)

Semester papers:

20 points

Oral exam:

55 points