Course code:
351H1		 Course name:
Selected Methods of Instrumental Analysis

Academic year:

2019/2020.

Attendance requirements:

There are no requirements.

ECTS:

9

Study level:

graduate academic studies, integrated basic and graduate academic studies

Study programs:

Chemical Education: 5. year, winter semester, elective (E5AP1) course

Chemistry: 1. year, winter semester, elective (E51H1) course

Environmental Chemistry: 1. year, winter semester, elective (E52S1) course

Teachers:

Rada M. Baošić, Ph.D.
full professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Tatjana Ž. Verbić, Ph.D.
associate professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Assistants:

Aleksandar Đ. Lolić, Ph.D.
full professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Miloš P. Pešić, Ph.D.
assistant with PhD, Faculty of Chemistry, Studentski trg 12-16, Beograd

Hours of instruction:

Weekly: four hours of lectures + two hours of exercises + three hours of labwork (4+2+3)

Goals:

Within the scope of the course students will complete their knowledge about various instrumental techniques that are used in analytical, environmental, pharmaceutical and medicinal chemistry.

Outcome:

Student will be qualified for independent research, optimisation and improving sensitivity of instrumental methods for the analysis of complex samples.

Teaching methods:

Lectures, labworks.

Extracurricular activities:

—

Coursebooks:

Main coursebooks:

  1. J.A.C. Broekaert: Analytic Atomic Spectroscopy with Flames and Plasmas, Willey, 2002
  2. J. Wang: Analytical Electrochemistry, Wiley, 2006
  3. A. J. Bard, L. R. Faulkner: Electrochemical methods, fundamentals and application, Willey, 2002
  4. J. Ruzicka, E. Hansen: Flow Injection Analysis, 2nd ed, Wiley Interscience
  5. F. Settle: Handbook of instrumental techniques for analytical chemistry, Prentice Hall PTR, Upper Saddle River, NJ 07458
  6. Z. Mandić - Ed: Physico-Chemical Methods in Drug Discovery and Development, IAPC Publishing, Zagreb, Croatia, 2012
  7. J. R. Lakowicz: Principles of Fluorescence Spectroscopy, third ed., Springer Science Business Media, New York, USA, 2006
  8. A. Avdeef: Absorption and Drug Development, Second Edition, Wiley-Interscience, Hoboken NJ. 2012.

Supplementary coursebooks:

  • T. Verbić, M. Pešić, N. Obradović, I. Cvijetić: Praktikum sa zbirkom zadataka iz instrumentalne analitičke hemije - optičke i elektroanalitičke metode, Univerzitet u Beogradu - Hemijski fakultet, 2018.

    Additional material:

    —

      Course activities and grading method

    Lectures:

    5 points (4 hours a week)

    Syllabus:

    • Modern optical methods, introduction
    • Atomic absorption and emission spectroscopy
    • Flow-injection analysis
    • Spectroelectrochemistry
    • Cyclic and stripping voltammetry
    • Pulse voltammetric techniques
    • Electrochemical sensors and electrode modifications
    • Electrochemical methods of separation
    • Hybrid techniques
    • Application of instrumental methods in environmental chemistry
    • Potentiometry, potentiometric titrations and potentiometric biosensors
    • Fluorescence spectroscopy (FS) - principles and application
    • Capillary electrophoresis (CE) - principles and application
    • Detection methods in liquid chromatography
    • Equilibria in analytical chemistry – methods for determination of dissociation constants, lipophilicity and solubility
    • Experimental techniques for measurements of plasma proteins – small molecules binding
    • Isothermal titration calorimetry (ITC) – principles and application
    • Surface plasmon resonance (SPR) - principles and application
    • Molecularly imprinted polymers (MIP)

    Exercises:

    0 points (2 hours a week)

    Labwork:

    20 points (3 hours a week)

    Semester papers:

    20 points

    Oral exam:

    55 points